2009, №3

pp. 3-6

The Development of Des-Glaucine Production Method in Subcritical Water Media

2009, №3

сс. 3-6

Quote

S.N. Borisenko, A.V. Bicherov, O.V. Pavluk, N.N. Kharabaev, N.I. Borisenko, E.V. Vetrova, V.I. Minkin, R.N. Borisenko, A.V. Lekar.

Key words: subcritical water, glaucine, des-glaucine, ESI-MS, NMR

The isomerization of non-racemic mixture of glaucine isomers into des-glaucine was held in subcritical water media under 200-300°С with the yeld 53 %. The structure of the product was proved with nuclear magnetic resonance spectroscopy (NMR) and electrospray ionization (ESI-MS).