Synthesis of Seco-Glaucine as a Model Study for Synthesis of Phenanthridone Alkaloids from Herbal Aporphine Alkaloids

2017, №2

сс. 19-25

E.V. Vetrova, S.V. Kurbatov, S.N. Borisenko, A.V. Lekar, S.S. Khizrieva, N.I. Borisenko, V.I. Minkin.

Key words: subcritical water, aporphine alkaloids, glaucine, phenanthrene alkaloids, seco-glaucine, HPLC

The synthesis of phenanthrene alkaloid seco-glaucine from herbal aporphine alkaloid glaucine in subcritical water is studied at 100—250 °C with no catalytic additived. The maximum product yield (∼ 80 %) that is reached at 250 °C is virtually independent on the amount of the initial compound. The product can be directly preci pitated from the reaction mixture if its concentration is sufficiently high. No use of constly and toxic organic solvents is required.

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ГОСТ
7.0.100-2018

Ветрова, Е.В. Synthesis of Seco-Glaucine as a Model Study for Synthesis of Phenanthridone Alkaloids from Herbal Aporphine Alkaloids / Е.В. Ветрова, С.В. Курбатов, С.Н. Борисенко [и др.]. – Текст : непосредственный // Сверхкритические Флюиды: Теория и Практика.. – 2017. – Т. 12. – № 2. – С. 19-25.

TRANSLIT

Vetrova, E.V. Sintez fenantrenovyh alkaloidov iz rastitel'nyh aporfinovyh alkaloidov v srede subkriticheskoj vody na primere polucheniya seko-glaucina / E.V. Vetrova, S.V. Kurbatov, S.N. Borisenko [i dr.]. – Tekst : neposredstvennyj // Sverhkriticheskie Flyuidy: Teoriya i Praktika.. – 2017. – Т. 12. – № 2. – S. 19-25.

E.V. Vetrova, S.V. Kurbatov, S.N. Borisenko, A.V. Lekar, S.S. Khizrieva, N.I. Borisenko, V.I. Minkin Synthesis of Seco-Glaucine as a Model Study for Synthesis of Phenanthridone Alkaloids from Herbal Aporphine Alkaloids. Sverhkriticheskie Flyuidy: Teoriya i Praktika, 2, 19-25 (2017). https://doi.org/

Synthesis of Seco-Glaucine as a Model Study for Synthesis of Phenanthridone Alkaloids from Herbal Aporphine Alkaloids

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