2025, №4

pp. 68-78

Mechanism of Calcium Stannates Crystallization in Sub- and Supercritical Water Fluid

2025, №4

сс. 68-78

Quote

D.K. Garanin, T.V. Bogdan, Yu.D. Ivakin, E.V. Tararushkin, V.I. Bogdan.

Key words: CaSn(OH)6, CaSnO3, solid-phase mobility, supercritical water fluid, molecular dynamic simulation, DFT

Unlike the traditional hydrothermal method, when the components interact in a solution, under processing a mixture of oxide powders in water vapor or supercritical fluid, the products are formed by solid-phase interaction of the reagents. Treatment of tin and calcium oxides in an autoclave under subcritical water vapour (270 °C) leads to the formation of CaSn(OH)6 crystals, and under supercritical water (400 °C) — to the formation of CaSnO3 crystals. The mechanism of solid-phase mobility during the formation of new phases in water fluid medium is discussed. The interaction of CaSn(OH)6 with water at 25 and 270 °C was simulated by molecular dynamics using DFT calculated potential function.

doi:10.34984/SCFTP.2025.20.4.007