2008, №4

сс. 66-82

The comparison of β-pinene reactivity in thermolysis at vapor-phase and supercritical conditions

2008, №4

сс. 66-82

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A.M. Chibiryaev, A. Yermakova, I.V. Kozhevnikov

Key words: thermolysis, supercritical ethanol, terpenes, β-pinene, β-myrcene, limonene, p-menthadiene, kinetic modeling, isokinetic relationship

For the first time the procedure for isolation of oil from Evening Primrose seeds using
        carbon dioxide Supercritical Fluid Extraction has been proposed. The process parameters
        as a function of pressure and temperature were studied. Qualitative and quantitative analysis
        of oil has been performed. The proposed method permits to produce oil of high quality
        without any traces of organic solvents which is ready for practical use excluding additional
        processing. In addition, the method of Accelerated Solvent Extraction (isopropanol) was
        used to utilize residual grist, which allows to isolate polar polyphenolic fraction.